Synthesis and optimization of experimental variables of a hybrid organic-inorganic compound

D. Contreras, Y. Moreno, Y. Salgado, G. Cárdenas, R. Baggio, O. Peña, J. Y. Pivan

Resultado de la investigación: Contribución a una revistaArtículo

10 Citas (Scopus)

Resumen

A multivariate study of the experimental parameters used in hydrothermal techniques (temperature, time, pH, relationship among reagents) was performed, and applied to the synthesis of a copper hybrid compound, [Cu(biqui)(H 2PO4)2]. In this way it was possible to rationalize the crystal yield and to find the best conditions to obtain the highest crystal production. The optimization was carried out through the Response Surface Method (RSM). The optimal values were determined over the response surface by the SIMPLEX method. These values were pH = 2.5, temperature = 123°C, time = 3.32 days and Cu(NO3)2 mass = 0.354 g. With these values the predicted crystal mass is 0.0376 ± 0.0082 g, considering the 95% of confidence interval.

Idioma originalInglés
Páginas (desde-hasta)1751-1754
Número de páginas4
PublicaciónNew Journal of Chemistry
Volumen31
N.º10
DOI
EstadoPublicada - 1 ene 2007

Áreas temáticas de ASJC Scopus

  • Catálisis
  • Química (todo)
  • Química de los materiales

Huella Profundice en los temas de investigación de 'Synthesis and optimization of experimental variables of a hybrid organic-inorganic compound'. En conjunto forman una huella única.

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    Contreras, D., Moreno, Y., Salgado, Y., Cárdenas, G., Baggio, R., Peña, O., & Pivan, J. Y. (2007). Synthesis and optimization of experimental variables of a hybrid organic-inorganic compound. New Journal of Chemistry, 31(10), 1751-1754. https://doi.org/10.1039/b703592f